Preparation and Structural Investigation of CuCl2 Graphite Intercalation Compounds
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Abstract:
Superfine graphite powder was prepared by ball-milling exfoliated graphite containing anhydrous CuCl2 in planetary ball milling systems. Nano-scale CuCl2 graphite intercalation compounds were synthesized by heating a mixture of anhydrous CuCl2 and graphite nanosheets. Scanning electron microscopy, energy-dispersive X-ray spectroscopy and high-resolution transmission electron microscopy were performed to characterize the microstructures of stage-1 nano-scale CuCl2 graphite intercalation compounds. The structure and components of the domain wall and core in the nano-scale CuCl2 graphite intercalation compounds are described. The results show that the content of CuCl2 in the mixture plays a crucial role in the size of the nano-scale CuCl2 graphite intercalation compound.
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Bin Xiaobei, Chen Jiazang, Cao Hong, Ma Enbao, Wang Xuehua, Yuan Jizhu.2008. Preparation and Structural Investigation of CuCl2 Graphite Intercalation Compounds[J]. Acta Geologica Sinica(),82(5):1056-1060