一件可能的Hf同位素测定标准锆石
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中国地质调查局地质调查项目


A Potential Standard Zircon for Hf Isotopic Analysis
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    摘要:

    陕西省西乡县汉南杂岩望江山岩体辉长岩中含有丰富的锆石——从600kg辉长岩样品中分选出结晶良好、内部结构简单、成因和年龄单一、Hf同位素比值均一的锆石7g,锆石粒度多为0.2-0.3mm。分别在三个不同实验室利用三种方法对该锆石样品进行了U-Pb同位素年龄测定,获得了在误差范围内完全一致的年龄:819.8 ± 2.5 Ma(LA-ICP-MS)、821.7 ± 1.7 Ma(LA-MC-ICPMS)和822.1 ± 4.5 Ma(SHRIMP)。在国内4个权威实验室对该锆石进行了Lu-Hf同位素测定,获得了在误差范围内完全一致的176Hf/177Hf同位素比值——全部421个测试点加权平均值为0.282535 ± 0.000003(2σ)。采样点岩体规模巨大,露头良好,岩石新鲜,交通方便。该锆石样品满足作为Hf同位素测定标样的各方面的指标,可能是一个比较理想的Hf 同位素测定标样。Hf同位素测定标准物质的研制,是测定获得准确可靠的Hf同位素数据的基础,具有十分重要的实用价值和科学意义。

    Abstract:

    It is discovered that the Wangjiangshan gabbro from the Hannan intrusive complex in the Xixiang County, Shaanxi Province contains abundant zircons; 7 g zircons, well-crystallized, simple in internal structure and origin, homogenious in U-Pb age and Hf isotopic composition, and with crystal size of 0.2 to 0.3 mm have been separated from 600 kg gabbro sample. U-Pb dating was carried out for the zircons using three different methods in three different laboratories; consistent ages were obtained: 819.8 ± 2.5 Ma (LA-ICP-MS), 821.7 ± 1.7 Ma (LA-MC-ICPMS) and 822.1 ± 4.5 Ma (SHRIMP). The Hf isotopic compositions of the zircons were measured in four authoritative laboratories and consistent 176Hf/177Hf ratios were obtained, the weighted average 176Hf/177Hf ratio of the total 421 analyses is 0.282535 ± 0.000003 (2σ). The sampled gabbro is well-outcropped, fresh, with large scale in smapling site, and convenient to access. Hence the zircons separated from the Wangjiangshan gabbro seem to meet the main requirements of Hf analysis standard; might serve as a standard zircon for Hf analysis. Hf isotopic standard preparation is to get accurate and reliable determination of Hf isotopic data ,and has very important practical value and scientific significance.

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周红英,李怀坤,耿建珍,苏文博,相振群,崔玉荣,张健,李惠民.2013.一件可能的Hf同位素测定标准锆石[J].地质学报,87(4):554-564.
ZHOU Hongying, LI Huaikun, GENG Jianzhen, SU Wenbo, XIANG Zhenqun, CUI Yurong, ZHANG Jian, LI Huimin.2013. A Potential Standard Zircon for Hf Isotopic Analysis[J]. Acta Geologica Sinica,87(4):554-564.

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  • 收稿日期:2012-09-07
  • 最后修改日期:2013-01-25
  • 录用日期:2013-04-15
  • 在线发布日期: 2013-04-22
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